反应在常温下进行,乙酰化产物的产率和质量与原方法相当。
The reaction proceeds at room temperature and the quality and yield of acetylate are comparison with ordinary method.
在有氢氧化钙存在时与2倍量的酰氯反应主要得到4 ,5 位酰化产物。
Acyl 5 acyloxypyrazoles were obtained with 2 equivalents of acid chlorides in the present of calcium hydroxide.
结果与结论:在该条件下水杨酸可以和DIPPH发生磷酰化反应,生成水杨酸羟基磷酰化产物。
Results and Conclusion: The phosphorylating reaction could happen under the condition mentioned between salicylic acid and phosphorylating agent-DIPPH. The target product could be determined by NMR.
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