微波技术应用于有机合成反应,反应速度比常规方法要加快数十甚至数千倍,并且能合成出常规方法难以生成的物质,正越来越广泛运用于材料,制药,化工及其他相关科研和教学领域。
Intellective microwave reactor、commercial microwave reactor and high efficiency microwave reactor were used, The effect of reaction time、reaction temperature、microwave power、raw material ratio、catalyst and solvent on reaction result were studied. The results were dissculed and analysed.
本文首先以邻氯苯酚为原料,在微波辐射下相转移催化合成邻乙氧基苯酚,分别使用智能型微波反应器、家用微波炉和高效微波消解系统,探索了原料摩尔比、反应时间、反应温度、微波功率、催化剂、溶剂以及溶剂量等因素对实验产物的影响,对实验结果进行了讨论和原因分析。
参考来源 - 对叔丁基邻苯二酚的合成研究·2,447,543篇论文数据,部分数据来源于NoteExpress
在微波反应器中以酸酯化-碱酯交换两步法制备生物柴油。
In a microwave reactor, the biological diesel oil is prepared from an acid esterification-alkali ester exchange two-step method.
针对微波有机合成反应技术及专用微波反应器作了重点介绍。
The reaction technique of microwave-assisted organic synthesis and the reaction-oriented special microwave equipment were analyzed in this paper.
在反应瓶中利用普通方法合成恶丙嗪和在微波反应器中利用微波辐射合成恶丙嗪。
Oxaprozine was synthesized by the microwave irradiation in microwave reaction instrument and by the common method in the flask.
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