分析了以草酸钠为基准物标定高锰酸钾标准溶液浓度的反应原理,标定操作及温度、酸度、滴定速度等滴定条件对标定结果的影响。
This paper discusses the reaction principle and titrimetric operation in defining consistency of potassium permanganate titrant which sodium oxalate is regarded as the basis material.
无需标准溶液的滴定计算分析能同时求出滴定剂与被测物质浓度。
The calculating analysis of titration without standard solution is a method that can be used to determine the concentration of substance titrated and titrant at the same time.
本文着重对分析测试中标准溶液浓度的选择、配制方法以及取样方式等细节问题提出了自己的见解。
The article put forwards the opinions on the selection of standard solution concentration, compound method and sample mode.
目的对按照2005年版《中国药典》方法配制和标定的盐酸标准溶液浓度进行不确定度评定。
Objective To evaluate uncertainty for concentration of hydrochloric acid standard solution prepared and standardized with the method in Chinese Pharmacopoeia (edition 2005).
利用标准溶液确定溶液的吸收系数,进而可以测量出未知溶液的浓度。
Standard liquid is used to determine the liquid absorbing coefficient so that the unknown liquid density is measured.
通过对全程序空白与已知浓度二氧化硫标准溶液的对照分析,提出了大气二氧化硫分析中质控图的做法。
Through the comparision between the blank and the sulfur dioxide standard solution, the way to make the sulfur dioxide quality control map is pointed out in the analysis of sulfur dioxide.
提出一种准确配制固定浓度标准溶液的方法。
The method which accurately prepared the standard solution of fixed concentration was suggested in this paper.
采用一个小锥形瓶固定其体积,便一定浓度的工作溶液添加数次便可获得一系列标准系列。
Use a conical flask to fix the volume, addition of a working solution of known concentration by several times can prepare a standard series.
根据FIA梯度稀释技术建立了一种新的标准加入方法,只需要注入一种标准溶液,就能形成浓度梯度。
Based on the gradient dilution technique of FIA, a new standard addition method is established. Concentration gradient can be formed by injection of only one single standard solution.
结果各种溶液测定的总标准差小于其浓度的5 %或检出限,总平均回收率可信限在允许范围内。
Results Total standard deviation of every solution was less than 5% of the concentration or detection limit. The confident limit of total average rate of recovery in sample kept in range of allowable.
该方法通过对初配的标准溶液进行两次浓度标度和一次调整,就可以达到所要求的标准溶液的浓度。方法简便,快速准确,具有实用性。
The standard solution of first preparation was calibrated twice and adjusted once respectly , then it could reach a required concentration of standard solution.
标准滴定溶液的标定是其浓度的量值溯源,GB/T 601–2002[1]通过规定工作基准试剂摩尔质量的有效数字,减少因数字修约而引入的不确定度。
Abstract It was commented on significant figures of mole mass of Zinc Oxide and relative atomic weight in calibrating for EDTA standard volumetric solution in GB/T 601–2002.
标准滴定溶液的标定是其浓度的量值溯源,GB/T 601–2002[1]通过规定工作基准试剂摩尔质量的有效数字,减少因数字修约而引入的不确定度。
Abstract It was commented on significant figures of mole mass of Zinc Oxide and relative atomic weight in calibrating for EDTA standard volumetric solution in GB/T 601–2002.
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